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Solid-State NMR by Paul Hodgkinson, Robin K. Harris, David C. Apperley

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CHAPTER 5

GOING FURTHER WITH SPIN-missing image file SOLID-STATE NMR

5.1 INTRODUCTION

The basic principles of solid-state NMR for dilute spin-missing image file nuclei, such as 13C and 15N, were set out in chapter 3. This chapter first considers how the basic techniques of Hartmann–Hahn cross-polarization (CP) and high-power proton decoupling need to be modified under the conditions of high magnetic fields and fast magic-angle spinning (MAS) rates which are now available and which are increasingly important for the study of complex systems, such as microcrystalline proteins.

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