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Solid-State NMR by Paul Hodgkinson, Robin K. Harris, David C. Apperley

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CHAPTER 3

SPIN-missing image file NUCLEI: A PRACTICAL GUIDE

3.1 INTRODUCTION

This chapter gives a beginner’s guide to the experimental solid-state NMR of spin-missing image file nuclei. It is a break from consideration of the underlying principles of solid-state NMR, concentrating instead on what it is necessary to know in order to obtain one-dimensional spectra, such as those shown in figure 3.1. These spectra are often valuable on their own and they are also the starting point for any of the more complex experiments described later on. Quadrupolar nuclei are treated separately ...

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